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This study aims to investigate the synergistic friction reduction and antiwear effects of lyophilized graphene loading nano-copper (RGO/Cu) as lubricating oil additives, compared with graphene.

The friction performance of freeze-drying graphene (RGO) and RGO/Cu particles was investigated at different addition concentrations and under different conditions.

Graphene plays a synergistic friction reduction and antiwear effect because of its large specific surface area, surface folds and loading capacity on the nanoparticles. The results showed that the average friction coefficients of RGO and RGO/Cu particles were 22.9% and 6.1% lower than that of base oil and RGO oil, respectively. In addition, the widths of wear scars were 62.3% and 55.3% lower than those of RGO/Cu particles, respectively.

The RGO single agent is suitable for medium-load and high-speed conditions, while the RGO/Cu particles can perform better in the conditions of heavy load and high speed.

The purpose of this paper is to enhance the characteristics of TiO₂ nanoparticles (NPs). Because these NPs stick together easily and are difficult to distribute evenly, they cannot be used extensively in lubricating oils. Altering TiO₂ was recommended as an alternate way for making NPs simpler to disperse.

Through dielectric barrier discharge plasma (DBDP)-assisted ball mill diagnostics and modeling of molecular dynamics, TiO₂@PEG-400 NPs were produced using the DBDP-assisted ball mill. The NPs’ microstructure was examined using FESEM, TEM, XRD, FT-IR and TG-DSC. Using the CFT-1 reciprocating friction tester, the tribological properties of TiO₂@PEG-400 NPs as base oil additives were studied. EDS and XPS were used to examine the surface wear of the friction pair.

Tribological properties of the modified NPs are vastly superior to those of the original NPs, and the lipophilicity value of TiO₂ NPs was improved by 200%. It was determined through tribological testing that TiO₂@PEG-400’s exceptional performance might be attributable to a chemical reaction film made up of TiO₂, Fe₂O₃, iron oxide and other organic chemicals.

This work describes an approach for preventing the aggregation of TiO₂ NPs by coating their surface with PEG-400. In addition, the prepared NPs can enhance the tribological performance of lubricating oil. This low-cost, high-performance lubricant additive has tremendous promise for usage in marine engines to minimize operating costs while preserving navigational safety.